SCALPEL 3D

i) TopSpin files
a) AU program: setscalpelpars
b) Pulse sequence for BRUKER: SCALPEL_it2
c) Pulse sequence for BRUKER: SCALPEL_idiff
d) Pulse sequence for BRUKER: gdp_2dsel_it2_dipsi
e) Pulse sequence for BRUKER: gdp_2dsel_idiff_dipsi

ii) SCALPEL data (BRUKER format)
a)Glucose, glucose-6-phosphate and maltose, in D2O
(FOLDER Glucose_gluc6P_maltose)
1 - 1H
2 - 2D 1H Oneshot45, with water pre-saturation
3 - 2D 1H iDESTO, with water pre-saturation
4 - 1H selective TOCSY
5 - 3D SCALPEL (using TOCSY-t1 and diffusion)

b)Lactose and melibiose, in D2O
(FOLDER Lactose_melibiose)
1 - 1H
2 - 2D 1H iREST2, with water pre-saturation
3 - 2D SCALPEL (first increment of TOCSY-t1 and relaxation decay), with water pre-saturation
4 - 3D SCALPEL (using TOCSY-t1 and relaxation), with water pre-saturation


c)Mackeson Stout, with 20% added D2O
(FOLDER Stout_20%D2O)
1 - 1H
2 - 2D 1H Oneshot45, with water pre-saturation
3 - 2D 1H iDESTO with, water pre-saturation
4 - 1H, with water pre-saturation
5 - {1H}13C
6 - 2D EA-HSQC
7 - 2D EA-HSQC-TOCSY
8 - 3D SCALPEL (using TOCSY-t1 and diffusion)
9 - 3D SCALPEL (using TOCSY-t1 and relaxation)
10 - 1H selective TOCSY
11 - 3D SCALPEL (using TOCSY-t1 and diffusion), with water pre-saturation