Comparative determination of the α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy

M M Attallah; S Zabeen; R J Cernik; M Preuss

doi:10.1016/j.matchar.2009.05.006

Comparative determination of the α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy

M M Attallah, S Zabeen, R J Cernik, M Preuss

Research output: Contribution to journal › Article › peer-review

Abstract

A comparison is made between the measured α/β phase fractions in Ti-6246 using X-ray diffraction (XRD) and electron microscopy. Image anal. of SEM and TEM images was compared to the phase fraction est. obtained using electron backscattered diffraction, lab and high-energy synchrotron XRD. There was a good agreement between the electron microscopic and diffraction techniques, provided that the microstructural parameters of grain size and texture are estd. correctly when using quant. Rietveld refinement. [on SciFinder(R)]

Original language	English
Pages (from-to)	1248-1256
Number of pages	9
Journal	Mater. Charact.
Volume	60
Issue number	11
DOIs	https://doi.org/10.1016/j.matchar.2009.05.006
Publication status	Published - 2009

Keywords

Electron diffraction
Grain size
Texture
X-ray diffractometry (comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy)
Metallography (electron
comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy)
titanium alloy alpha beta phase fraction microscopy diffractometry

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10.1016/j.matchar.2009.05.006

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@article{b9b795ab477e472ba0097dcecec5e8e6,

title = "Comparative determination of the α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy",

abstract = "A comparison is made between the measured α/β phase fractions in Ti-6246 using X-ray diffraction (XRD) and electron microscopy. Image anal. of SEM and TEM images was compared to the phase fraction est. obtained using electron backscattered diffraction, lab and high-energy synchrotron XRD. There was a good agreement between the electron microscopic and diffraction techniques, provided that the microstructural parameters of grain size and texture are estd. correctly when using quant. Rietveld refinement. [on SciFinder(R)]",

keywords = "Electron diffraction, Grain size, Texture, X-ray diffractometry (comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy), Metallography (electron, comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy), titanium alloy alpha beta phase fraction microscopy diffractometry",

author = "Attallah, {M M} and S Zabeen and Cernik, {R J} and M Preuss",

note = "CAN 152:268520 Nonferrous Metals and Alloys 52293-96-6 (Ti6Al2Sn4Zr6Mo) Role: PEP (Physical, engineering or chemical process), PRP (Properties), PROC (Process) (comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy)",

year = "2009",

doi = "10.1016/j.matchar.2009.05.006",

language = "English",

volume = "60",

pages = "1248--1256",

journal = "Mater. Charact.",

issn = "1044-5803",

publisher = "Elsevier BV",

number = "11",

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TY - JOUR

T1 - Comparative determination of the α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy

AU - Attallah, M M

AU - Zabeen, S

AU - Cernik, R J

AU - Preuss, M

N1 - CAN 152:268520 Nonferrous Metals and Alloys 52293-96-6 (Ti6Al2Sn4Zr6Mo) Role: PEP (Physical, engineering or chemical process), PRP (Properties), PROC (Process) (comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy)

PY - 2009

Y1 - 2009

N2 - A comparison is made between the measured α/β phase fractions in Ti-6246 using X-ray diffraction (XRD) and electron microscopy. Image anal. of SEM and TEM images was compared to the phase fraction est. obtained using electron backscattered diffraction, lab and high-energy synchrotron XRD. There was a good agreement between the electron microscopic and diffraction techniques, provided that the microstructural parameters of grain size and texture are estd. correctly when using quant. Rietveld refinement. [on SciFinder(R)]

AB - A comparison is made between the measured α/β phase fractions in Ti-6246 using X-ray diffraction (XRD) and electron microscopy. Image anal. of SEM and TEM images was compared to the phase fraction est. obtained using electron backscattered diffraction, lab and high-energy synchrotron XRD. There was a good agreement between the electron microscopic and diffraction techniques, provided that the microstructural parameters of grain size and texture are estd. correctly when using quant. Rietveld refinement. [on SciFinder(R)]

KW - Electron diffraction

KW - Grain size

KW - Texture

KW - X-ray diffractometry (comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy)

KW - Metallography (electron

KW - comparative detn. of α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy)

KW - titanium alloy alpha beta phase fraction microscopy diffractometry

U2 - 10.1016/j.matchar.2009.05.006

DO - 10.1016/j.matchar.2009.05.006

M3 - Article

SN - 1044-5803

VL - 60

SP - 1248

EP - 1256

JO - Mater. Charact.

JF - Mater. Charact.

IS - 11

ER -

Comparative determination of the α/β phase fraction in α+β-titanium alloys using X-ray diffraction and electron microscopy

Abstract

Keywords

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