Deposition of iron selenide nanocrystals and thin films from tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii)

Masood Akhtar; Javeed Akhtar; Mohammad Azad Malik; Floriana Tuna; Madeleine Helliwell; Paul O'Brien

doi:10.1039/c2jm31291c

Deposition of iron selenide nanocrystals and thin films from tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii)

Masood Akhtar, Javeed Akhtar, Mohammad Azad Malik, Floriana Tuna, Madeleine Helliwell, Paul O'Brien

Research output: Contribution to journal › Article › peer-review

Abstract

The complex tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii) was synthesised and its X-ray single crystal structure determined. Thermolysis of this complex in oleylamine at all temperatures produced nanocrystals of FeSe 2 whereas Aerosol Assisted Chemical Vapour Deposition produced FeSe thin films on silicon substrates. Nanocrystals and thin films were characterised by powder X-ray diffraction (p-XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), and transmission electron microscopy (TEM). This journal is © The Royal Society of Chemistry 2012.

Original language	English
Pages (from-to)	14970-14975
Number of pages	5
Journal	Journal of Materials Chemistry
Volume	22
Issue number	30
DOIs	https://doi.org/10.1039/c2jm31291c
Publication status	Published - 14 Aug 2012

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10.1039/c2jm31291c

CCDC 776130: Experimental Crystal Structure Determination
Akhtar, J. (Contributor), Akhtar, J. (Contributor), Malik, M. (Contributor), Tuna, F. (Contributor), Helliwell, M. (Contributor) & O'Brien, P. (Contributor), Cambridge Crystallographic Data Centre, 1 Jan 2012
DOI: 10.5517/ccv1mgy, http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccv1mgy&sid=DataCite
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title = "Deposition of iron selenide nanocrystals and thin films from tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii)",

abstract = "The complex tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii) was synthesised and its X-ray single crystal structure determined. Thermolysis of this complex in oleylamine at all temperatures produced nanocrystals of FeSe 2 whereas Aerosol Assisted Chemical Vapour Deposition produced FeSe thin films on silicon substrates. Nanocrystals and thin films were characterised by powder X-ray diffraction (p-XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), and transmission electron microscopy (TEM). This journal is {\textcopyright} The Royal Society of Chemistry 2012.",

author = "Masood Akhtar and Javeed Akhtar and Malik, {Mohammad Azad} and Floriana Tuna and Madeleine Helliwell and Paul O'Brien",

year = "2012",

month = aug,

day = "14",

doi = "10.1039/c2jm31291c",

language = "English",

volume = "22",

pages = "14970--14975",

journal = "Journal of Materials Chemistry",

issn = "1364-5501",

publisher = "Royal Society of Chemistry",

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TY - JOUR

T1 - Deposition of iron selenide nanocrystals and thin films from tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii)

AU - Akhtar, Masood

AU - Akhtar, Javeed

AU - Malik, Mohammad Azad

AU - Tuna, Floriana

AU - Helliwell, Madeleine

AU - O'Brien, Paul

PY - 2012/8/14

Y1 - 2012/8/14

N2 - The complex tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii) was synthesised and its X-ray single crystal structure determined. Thermolysis of this complex in oleylamine at all temperatures produced nanocrystals of FeSe 2 whereas Aerosol Assisted Chemical Vapour Deposition produced FeSe thin films on silicon substrates. Nanocrystals and thin films were characterised by powder X-ray diffraction (p-XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), and transmission electron microscopy (TEM). This journal is © The Royal Society of Chemistry 2012.

AB - The complex tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii) was synthesised and its X-ray single crystal structure determined. Thermolysis of this complex in oleylamine at all temperatures produced nanocrystals of FeSe 2 whereas Aerosol Assisted Chemical Vapour Deposition produced FeSe thin films on silicon substrates. Nanocrystals and thin films were characterised by powder X-ray diffraction (p-XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), and transmission electron microscopy (TEM). This journal is © The Royal Society of Chemistry 2012.

U2 - 10.1039/c2jm31291c

DO - 10.1039/c2jm31291c

M3 - Article

SN - 1364-5501

VL - 22

SP - 14970

EP - 14975

JO - Journal of Materials Chemistry

JF - Journal of Materials Chemistry

IS - 30

ER -

Deposition of iron selenide nanocrystals and thin films from tris(N,N-diethyl-N′-naphthoylselenoureato)iron(iii)

Abstract

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CCDC 776130: Experimental Crystal Structure Determination

Cite this