Dynamics and control of a heat pump assisted azeotropic dividing-wall column (HP-A-DWC) for biobutanol purification

Iulian Patraşcu, Costin Sorin Bîldea, Anton A. Kiss

    Research output: Chapter in Book/Report/Conference proceedingChapterpeer-review

    Abstract

    Recently, the butanol purification from acetone-butanol-ethanol mixture was achieved in one azeotropic dividing-wall column requiring 2.7 MJ/kg butanol, which represents just 7.5% of the energy content of butanol. Compared to a conventional separation sequence, this design allows 60% energy savings due to heat integration and use of a heat pump. This work considers the dynamics and control of the process. The basic regulatory control can provide stability for small and short-time disturbances, but the process shuts down if the disturbances persist. By adding a reboiler and a condenser, better control becomes possible. As a result, the process can handle large and persistent disturbances in feed rate and composition, achieving good control of product purity.

    Original languageEnglish
    Title of host publicationComputer Aided Chemical Engineering
    PublisherElsevier BV
    Pages1339-1344
    Number of pages6
    DOIs
    Publication statusPublished - 2019

    Publication series

    NameComputer Aided Chemical Engineering
    Volume46
    ISSN (Print)1570-7946

    Keywords

    • Dividing-wall column
    • heat integration
    • optimal design
    • process control

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