Enhanced resin titanium adhesion with silane primers using tribochemical silica-coating

Aftab Ahmed Khan; Abdulaziz Abdullah Al Kheraif; Jamaluddin Syed; Darshan Devang Divakar; Jukka Pekka Matinlinna

doi:10.4012/dmj.2016-142

Enhanced resin titanium adhesion with silane primers using tribochemical silica-coating

Aftab Ahmed Khan
, Abdulaziz Abdullah Al Kheraif
, Jamaluddin Syed
, Darshan Devang Divakar
, Jukka Pekka Matinlinna

Research output: Contribution to journal › Article › peer-review

Abstract

Experimental silane primers and a urethane dimethacrylate resin were prepared to resin titanium bonding. Commercially pure 2 Ti coupons were pretreated and randomly assigned into groups: group-SM (ESPE Sil™+Multilink® Speed), group-SE (ESPE Sil™+experimental resin), group-AM (1.0 vol% 3-acryloxypropyltrimethoxysilane+Multilink® Speed), group-AE (1.0 vol% 3-acryloxypropyltrimethoxysilane+experimental resin), group-BM (1.0 vol% 3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl)ethane+Multilink® Speed), and group-BE (1.0 vol% 3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl) ethane+experimental resin). Specimens were stored in a desiccator for 24 h, and artificially aged by thermo-cycling (6,000 and 12,000 cycles). According to ANOVA and the Tukey's test (n=10, α=0.05), the mean enclosed mold shear bond strength after 24 h was highest in group-AE (26.2±4.0 MPa). After 12,000 thermo-cycles, the group-BM exhibited the highest adhesion strength (13.4±3.2 MPa). This study suggests that a silane primer (3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl)ethane) might enhance adhesion strength.

Original language	English
Pages (from-to)	111-116
Number of pages	6
Journal	Dental Materials Journal
Volume	36
Issue number	1
DOIs	https://doi.org/10.4012/dmj.2016-142
Publication status	Published - 31 Jan 2017

Keywords

Coated Materials, Biocompatible
Dental Bonding
Humans
Materials Testing
Resin Cements
Shear Strength
Silanes
Silicon Dioxide
Surface Properties
Titanium

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10.4012/dmj.2016-142

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title = "Enhanced resin titanium adhesion with silane primers using tribochemical silica-coating",

abstract = "Experimental silane primers and a urethane dimethacrylate resin were prepared to resin titanium bonding. Commercially pure 2 Ti coupons were pretreated and randomly assigned into groups: group-SM (ESPE Sil{\texttrademark}+Multilink{\textregistered} Speed), group-SE (ESPE Sil{\texttrademark}+experimental resin), group-AM (1.0 vol\% 3-acryloxypropyltrimethoxysilane+Multilink{\textregistered} Speed), group-AE (1.0 vol\% 3-acryloxypropyltrimethoxysilane+experimental resin), group-BM (1.0 vol\% 3-acryloxypropyltrimethoxysilane+0.5 vol\% bis-(1,2-triethoxysilyl)ethane+Multilink{\textregistered} Speed), and group-BE (1.0 vol\% 3-acryloxypropyltrimethoxysilane+0.5 vol\% bis-(1,2-triethoxysilyl) ethane+experimental resin). Specimens were stored in a desiccator for 24 h, and artificially aged by thermo-cycling (6,000 and 12,000 cycles). According to ANOVA and the Tukey's test (n=10, α=0.05), the mean enclosed mold shear bond strength after 24 h was highest in group-AE (26.2±4.0 MPa). After 12,000 thermo-cycles, the group-BM exhibited the highest adhesion strength (13.4±3.2 MPa). This study suggests that a silane primer (3-acryloxypropyltrimethoxysilane+0.5 vol\% bis-(1,2-triethoxysilyl)ethane) might enhance adhesion strength.",

keywords = "Coated Materials, Biocompatible, Dental Bonding, Humans, Materials Testing, Resin Cements, Shear Strength, Silanes, Silicon Dioxide, Surface Properties, Titanium",

author = "Khan, \{Aftab Ahmed\} and \{Al Kheraif\}, \{Abdulaziz Abdullah\} and Jamaluddin Syed and Divakar, \{Darshan Devang\} and Matinlinna, \{Jukka Pekka\}",

year = "2017",

month = jan,

day = "31",

doi = "10.4012/dmj.2016-142",

language = "English",

volume = "36",

pages = "111--116",

journal = "Dental Materials Journal",

issn = "0287-4547",

publisher = "Japanese Society for Dental Materials and Devices",

number = "1",

}

TY - JOUR

T1 - Enhanced resin titanium adhesion with silane primers using tribochemical silica-coating

AU - Khan, Aftab Ahmed

AU - Al Kheraif, Abdulaziz Abdullah

AU - Syed, Jamaluddin

AU - Divakar, Darshan Devang

AU - Matinlinna, Jukka Pekka

PY - 2017/1/31

Y1 - 2017/1/31

N2 - Experimental silane primers and a urethane dimethacrylate resin were prepared to resin titanium bonding. Commercially pure 2 Ti coupons were pretreated and randomly assigned into groups: group-SM (ESPE Sil™+Multilink® Speed), group-SE (ESPE Sil™+experimental resin), group-AM (1.0 vol% 3-acryloxypropyltrimethoxysilane+Multilink® Speed), group-AE (1.0 vol% 3-acryloxypropyltrimethoxysilane+experimental resin), group-BM (1.0 vol% 3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl)ethane+Multilink® Speed), and group-BE (1.0 vol% 3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl) ethane+experimental resin). Specimens were stored in a desiccator for 24 h, and artificially aged by thermo-cycling (6,000 and 12,000 cycles). According to ANOVA and the Tukey's test (n=10, α=0.05), the mean enclosed mold shear bond strength after 24 h was highest in group-AE (26.2±4.0 MPa). After 12,000 thermo-cycles, the group-BM exhibited the highest adhesion strength (13.4±3.2 MPa). This study suggests that a silane primer (3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl)ethane) might enhance adhesion strength.

AB - Experimental silane primers and a urethane dimethacrylate resin were prepared to resin titanium bonding. Commercially pure 2 Ti coupons were pretreated and randomly assigned into groups: group-SM (ESPE Sil™+Multilink® Speed), group-SE (ESPE Sil™+experimental resin), group-AM (1.0 vol% 3-acryloxypropyltrimethoxysilane+Multilink® Speed), group-AE (1.0 vol% 3-acryloxypropyltrimethoxysilane+experimental resin), group-BM (1.0 vol% 3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl)ethane+Multilink® Speed), and group-BE (1.0 vol% 3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl) ethane+experimental resin). Specimens were stored in a desiccator for 24 h, and artificially aged by thermo-cycling (6,000 and 12,000 cycles). According to ANOVA and the Tukey's test (n=10, α=0.05), the mean enclosed mold shear bond strength after 24 h was highest in group-AE (26.2±4.0 MPa). After 12,000 thermo-cycles, the group-BM exhibited the highest adhesion strength (13.4±3.2 MPa). This study suggests that a silane primer (3-acryloxypropyltrimethoxysilane+0.5 vol% bis-(1,2-triethoxysilyl)ethane) might enhance adhesion strength.

KW - Coated Materials, Biocompatible

KW - Dental Bonding

KW - Humans

KW - Materials Testing

KW - Resin Cements

KW - Shear Strength

KW - Silanes

KW - Silicon Dioxide

KW - Surface Properties

KW - Titanium

U2 - 10.4012/dmj.2016-142

DO - 10.4012/dmj.2016-142

M3 - Article

C2 - 28111386

SN - 0287-4547

VL - 36

SP - 111

EP - 116

JO - Dental Materials Journal

JF - Dental Materials Journal

IS - 1

ER -

Enhanced resin titanium adhesion with silane primers using tribochemical silica-coating

Abstract

Keywords

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