Measuring Couplings in Crowded NMR Spectra: Pure Shift NMR with Multiplet Analysis

Mohammadali Foroozandeh; RW Adams; Peter Kiraly; Mathias Nilsson; Gareth Morris

doi:10.1039/C5CC06293D

Measuring Couplings in Crowded NMR Spectra: Pure Shift NMR with Multiplet Analysis

Mohammadali Foroozandeh, RW Adams, Peter Kiraly, Mathias Nilsson, Gareth Morris

Research output: Contribution to journal › Article › peer-review

Abstract

The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin–spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.

Original language	English
Pages (from-to)	15410-15413
Number of pages	4
Journal	Chemical Communications
Volume	51
Issue number	84
DOIs	https://doi.org/10.1039/C5CC06293D
Publication status	Published - 27 Aug 2015

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title = "Measuring Couplings in Crowded NMR Spectra: Pure Shift NMR with Multiplet Analysis",

abstract = "The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin–spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.",

author = "Mohammadali Foroozandeh and RW Adams and Peter Kiraly and Mathias Nilsson and Gareth Morris",

year = "2015",

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doi = "10.1039/C5CC06293D",

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AU - Nilsson, Mathias

AU - Morris, Gareth

PY - 2015/8/27

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AB - The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin–spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.

U2 - 10.1039/C5CC06293D

DO - 10.1039/C5CC06293D

M3 - Article

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VL - 51

SP - 15410

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JO - Chemical Communications

JF - Chemical Communications

IS - 84

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Measuring Couplings in Crowded NMR Spectra: Pure Shift NMR with Multiplet Analysis

Abstract

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