N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen

R. Eric Banks; Mohamed K. Besheesh; Robin G. Pritchard

doi:10.1107/S0108270103001689

N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen

R. Eric Banks
, Mohamed K. Besheesh
, Robin G. Pritchard

Research output: Contribution to journal › Article › peer-review

Abstract

The molecular structures of N-fluoropyridinium trifluoromethanesulfonate (I) and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate (II) were analyzed. The N-F bond lengths in (I) and (II) were found to be 1.357 (4) and 1.354 (4) Ä respectively. The two structures were also found to differ in their crystal packing.

Original language	English
Pages (from-to)	m141-m143
Journal	Acta Crystallographica Section C: Crystal Structure Communications
Volume	59
Issue number	4
DOIs	https://doi.org/10.1107/S0108270103001689
Publication status	Published - Apr 2003

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Banks, R. E., Besheesh, M. K., & Pritchard, R. G. (2003). N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen. Acta Crystallographica Section C: Crystal Structure Communications, 59(4), m141-m143. https://doi.org/10.1107/S0108270103001689

Banks, R. Eric ; Besheesh, Mohamed K. ; Pritchard, Robin G. / N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen. In: Acta Crystallographica Section C: Crystal Structure Communications. 2003 ; Vol. 59, No. 4. pp. m141-m143.

@article{70b9ce2418ff4004b816273ed5b671ea,

title = "N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen",

abstract = "The molecular structures of N-fluoropyridinium trifluoromethanesulfonate (I) and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate (II) were analyzed. The N-F bond lengths in (I) and (II) were found to be 1.357 (4) and 1.354 (4) {\"A} respectively. The two structures were also found to differ in their crystal packing.",

author = "Banks, \{R. Eric\} and Besheesh, \{Mohamed K.\} and Pritchard, \{Robin G.\}",

year = "2003",

month = apr,

doi = "10.1107/S0108270103001689",

language = "English",

volume = "59",

pages = "m141--m143",

journal = "Acta Crystallographica Section C: Crystal Structure Communications",

issn = "0108-2701",

publisher = "International Union of Crystallography",

number = "4",

}

Banks, RE, Besheesh, MK & Pritchard, RG 2003, 'N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen', Acta Crystallographica Section C: Crystal Structure Communications, vol. 59, no. 4, pp. m141-m143. https://doi.org/10.1107/S0108270103001689

N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen. / Banks, R. Eric; Besheesh, Mohamed K.; Pritchard, Robin G.
In: Acta Crystallographica Section C: Crystal Structure Communications, Vol. 59, No. 4, 04.2003, p. m141-m143.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen

AU - Banks, R. Eric

AU - Besheesh, Mohamed K.

AU - Pritchard, Robin G.

PY - 2003/4

Y1 - 2003/4

N2 - The molecular structures of N-fluoropyridinium trifluoromethanesulfonate (I) and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate (II) were analyzed. The N-F bond lengths in (I) and (II) were found to be 1.357 (4) and 1.354 (4) Ä respectively. The two structures were also found to differ in their crystal packing.

AB - The molecular structures of N-fluoropyridinium trifluoromethanesulfonate (I) and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate (II) were analyzed. The N-F bond lengths in (I) and (II) were found to be 1.357 (4) and 1.354 (4) Ä respectively. The two structures were also found to differ in their crystal packing.

U2 - 10.1107/S0108270103001689

DO - 10.1107/S0108270103001689

M3 - Article

SN - 0108-2701

VL - 59

SP - m141-m143

JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

IS - 4

ER -

N-fluoropyridinium trifluoromethanesulfonate and 1-fluoro-2,4,6-trimethoxy-1,3,5-triazinium hexafluoroantimonate: The first experimental determination of the F-N+ bond length involving sp2 nitrogen

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