Neutron diffraction at simultaneous high temperatures and pressures, with measurement of temperature by neutron radiography

Y. Le Godec; M. T. Dove; D. J. Francis; S. C. Kohn; W. G. Marshall; A. R. Pawley; G. D. Price; S. A T Redfern; N. Rhodes; N. L. Ross; P. F. Schofield; E. Schooneveld; G. Syfosse; M. G. Tucker; M. D. Welch

doi:10.1180/0026461016560005

Neutron diffraction at simultaneous high temperatures and pressures, with measurement of temperature by neutron radiography

Y. Le Godec, M. T. Dove, D. J. Francis, S. C. Kohn, W. G. Marshall, A. R. Pawley, G. D. Price, S. A T Redfern, N. Rhodes, N. L. Ross, P. F. Schofield, E. Schooneveld, G. Syfosse, M. G. Tucker, M. D. Welch

Research output: Contribution to journal › Article › peer-review

Abstract

The commissioning and operation of apparatus for neutron diffraction at simultaneous high temperatures and pressures is reported. The basic design is based on the Paris-Edinburgh cell using opposed anvils, with internal heating. Temperature is measured using neutron radiography. The apparatus has been shown in both on-line and off-line tests to operate to a pressure of 7 GPa and temperature of 1700°C. The apparatus has been used in a neutron diffraction study of the crystal structure of deuterated brucite, and results for 520°C and 5.15 GPa are presented. The diffraction data that can be obtained from the apparatus are of comparable quality to previous high-pressure studies at ambient temperatures, and are clearly good enough for Rietveld refinement analysis to give structural data of reasonable quality.

Original language	English
Pages (from-to)	737-748
Number of pages	11
Journal	Mineralogical Magazine
Volume	65
Issue number	6
DOIs	https://doi.org/10.1180/0026461016560005
Publication status	Published - Dec 2001

Keywords

High pressure
High temperature
Neutron diffraction
Neutron radiography
Rietveld refinement

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10.1180/0026461016560005

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Le Godec, Y., Dove, M. T., Francis, D. J., Kohn, S. C., Marshall, W. G., Pawley, A. R., Price, G. D., Redfern, S. A. T., Rhodes, N., Ross, N. L., Schofield, P. F., Schooneveld, E., Syfosse, G., Tucker, M. G., & Welch, M. D. (2001). Neutron diffraction at simultaneous high temperatures and pressures, with measurement of temperature by neutron radiography. Mineralogical Magazine, 65(6), 737-748. https://doi.org/10.1180/0026461016560005

@article{2e3372c23b5447d2a295e79747fad61b,

title = "Neutron diffraction at simultaneous high temperatures and pressures, with measurement of temperature by neutron radiography",

abstract = "The commissioning and operation of apparatus for neutron diffraction at simultaneous high temperatures and pressures is reported. The basic design is based on the Paris-Edinburgh cell using opposed anvils, with internal heating. Temperature is measured using neutron radiography. The apparatus has been shown in both on-line and off-line tests to operate to a pressure of 7 GPa and temperature of 1700°C. The apparatus has been used in a neutron diffraction study of the crystal structure of deuterated brucite, and results for 520°C and 5.15 GPa are presented. The diffraction data that can be obtained from the apparatus are of comparable quality to previous high-pressure studies at ambient temperatures, and are clearly good enough for Rietveld refinement analysis to give structural data of reasonable quality.",

keywords = "High pressure, High temperature, Neutron diffraction, Neutron radiography, Rietveld refinement",

author = "{Le Godec}, Y. and Dove, {M. T.} and Francis, {D. J.} and Kohn, {S. C.} and Marshall, {W. G.} and Pawley, {A. R.} and Price, {G. D.} and Redfern, {S. A T} and N. Rhodes and Ross, {N. L.} and Schofield, {P. F.} and E. Schooneveld and G. Syfosse and Tucker, {M. G.} and Welch, {M. D.}",

year = "2001",

month = dec,

doi = "10.1180/0026461016560005",

language = "English",

volume = "65",

pages = "737--748",

journal = "Mineralogical Magazine",

issn = "1471-8022",

publisher = "Mineralogical Society",

number = "6",

}

Le Godec, Y, Dove, MT, Francis, DJ, Kohn, SC, Marshall, WG, Pawley, AR, Price, GD, Redfern, SAT, Rhodes, N, Ross, NL, Schofield, PF, Schooneveld, E, Syfosse, G, Tucker, MG & Welch, MD 2001, 'Neutron diffraction at simultaneous high temperatures and pressures, with measurement of temperature by neutron radiography', Mineralogical Magazine, vol. 65, no. 6, pp. 737-748. https://doi.org/10.1180/0026461016560005

TY - JOUR

T1 - Neutron diffraction at simultaneous high temperatures and pressures, with measurement of temperature by neutron radiography

AU - Le Godec, Y.

AU - Dove, M. T.

AU - Francis, D. J.

AU - Kohn, S. C.

AU - Marshall, W. G.

AU - Pawley, A. R.

AU - Price, G. D.

AU - Redfern, S. A T

AU - Rhodes, N.

AU - Ross, N. L.

AU - Schofield, P. F.

AU - Schooneveld, E.

AU - Syfosse, G.

AU - Tucker, M. G.

AU - Welch, M. D.

PY - 2001/12

Y1 - 2001/12

N2 - The commissioning and operation of apparatus for neutron diffraction at simultaneous high temperatures and pressures is reported. The basic design is based on the Paris-Edinburgh cell using opposed anvils, with internal heating. Temperature is measured using neutron radiography. The apparatus has been shown in both on-line and off-line tests to operate to a pressure of 7 GPa and temperature of 1700°C. The apparatus has been used in a neutron diffraction study of the crystal structure of deuterated brucite, and results for 520°C and 5.15 GPa are presented. The diffraction data that can be obtained from the apparatus are of comparable quality to previous high-pressure studies at ambient temperatures, and are clearly good enough for Rietveld refinement analysis to give structural data of reasonable quality.

AB - The commissioning and operation of apparatus for neutron diffraction at simultaneous high temperatures and pressures is reported. The basic design is based on the Paris-Edinburgh cell using opposed anvils, with internal heating. Temperature is measured using neutron radiography. The apparatus has been shown in both on-line and off-line tests to operate to a pressure of 7 GPa and temperature of 1700°C. The apparatus has been used in a neutron diffraction study of the crystal structure of deuterated brucite, and results for 520°C and 5.15 GPa are presented. The diffraction data that can be obtained from the apparatus are of comparable quality to previous high-pressure studies at ambient temperatures, and are clearly good enough for Rietveld refinement analysis to give structural data of reasonable quality.

KW - High pressure

KW - High temperature

KW - Neutron diffraction

KW - Neutron radiography

KW - Rietveld refinement

U2 - 10.1180/0026461016560005

DO - 10.1180/0026461016560005

M3 - Article

SN - 1471-8022

VL - 65

SP - 737

EP - 748

JO - Mineralogical Magazine

JF - Mineralogical Magazine

IS - 6

ER -

Neutron diffraction at simultaneous high temperatures and pressures, with measurement of temperature by neutron radiography

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