Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A

Stephen Bauters; Pieter Tack; Jennifer Rudloff-Grund; Dipanjan Banerjee; Allessandro Longo; Roelof Van Silfhout; Laszlo Vincze

doi:10.1021/acs.analchem.7b05110

Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A

Stephen Bauters, Pieter Tack, Jennifer Rudloff-Grund, Dipanjan Banerjee, Allessandro Longo, Roelof Van Silfhout, Laszlo Vincze

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Abstract

A novel plug-and-play setup based on polycapillary X-ray optics enables three-dimensional (3D) confocal X-ray fluorescence (XRF) and X-ray absorption spectroscopy down to 8 × 8 × 11 μm3 (17 keV) at the European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A. A complete description and analytical characterization is presented, together with two recently performed experimental cases. In Deep Earth diamond São Luiz-Frankfurt am Main 16, an olivine-rich inclusion was mapped with full 3D XRF elemental imaging. The preliminary tests on Iron Gall ink contained in an historical document, a letter from the court of King Philip II of Spain, reveal both the delicate nature of Iron Gall ink and the lack of Fe–Ni chemical bonding.

Original language	English
Pages (from-to)	2389-2394
Number of pages	6
Journal	Analytical Chemistry
Volume	90
Issue number	3
Early online date	10 Jan 2018
DOIs	https://doi.org/10.1021/acs.analchem.7b05110
Publication status	Published - 6 Feb 2018

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Bauters, S., Tack, P., Rudloff-Grund, J., Banerjee, D., Longo, A., Van Silfhout, R., & Vincze, L. (2018). Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A. Analytical Chemistry, 90(3), 2389-2394. https://doi.org/10.1021/acs.analchem.7b05110

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title = "Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A",

abstract = "A novel plug-and-play setup based on polycapillary X-ray optics enables three-dimensional (3D) confocal X-ray fluorescence (XRF) and X-ray absorption spectroscopy down to 8 × 8 × 11 μm3 (17 keV) at the European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A. A complete description and analytical characterization is presented, together with two recently performed experimental cases. In Deep Earth diamond S{\~a}o Luiz-Frankfurt am Main 16, an olivine-rich inclusion was mapped with full 3D XRF elemental imaging. The preliminary tests on Iron Gall ink contained in an historical document, a letter from the court of King Philip II of Spain, reveal both the delicate nature of Iron Gall ink and the lack of Fe–Ni chemical bonding.",

author = "Stephen Bauters and Pieter Tack and Jennifer Rudloff-Grund and Dipanjan Banerjee and Allessandro Longo and {Van Silfhout}, Roelof and Laszlo Vincze",

note = "Funding Information: We would like to acknowledge Frederik Muller for providing the letter originating from the court of King Philip II of Spain and Daniel Michon (Artechnique) for the professional photoshoot of the setup as seen in Figure 1. Dirk Detollenaere and Florian Ledrappier from the DUBBLE are thanked for their extensive support during development and construction. The authors acknowledge the financial support by the Research Foundation - Flanders (FWO) via Big Science project nr. G.0C12.13. Publisher Copyright: {\textcopyright} 2018 American Chemical Society. Copyright: Copyright 2018 Elsevier B.V., All rights reserved.",

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doi = "10.1021/acs.analchem.7b05110",

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Bauters, S, Tack, P, Rudloff-Grund, J, Banerjee, D, Longo, A, Van Silfhout, R & Vincze, L 2018, 'Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A', Analytical Chemistry, vol. 90, no. 3, pp. 2389-2394. https://doi.org/10.1021/acs.analchem.7b05110

Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A. / Bauters, Stephen; Tack, Pieter; Rudloff-Grund, Jennifer et al.
In: Analytical Chemistry, Vol. 90, No. 3, 06.02.2018, p. 2389-2394.

Research output: Contribution to journal › Article › peer-review

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AU - Rudloff-Grund, Jennifer

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AU - Longo, Allessandro

AU - Van Silfhout, Roelof

AU - Vincze, Laszlo

N1 - Funding Information: We would like to acknowledge Frederik Muller for providing the letter originating from the court of King Philip II of Spain and Daniel Michon (Artechnique) for the professional photoshoot of the setup as seen in Figure 1. Dirk Detollenaere and Florian Ledrappier from the DUBBLE are thanked for their extensive support during development and construction. The authors acknowledge the financial support by the Research Foundation - Flanders (FWO) via Big Science project nr. G.0C12.13. Publisher Copyright: © 2018 American Chemical Society. Copyright: Copyright 2018 Elsevier B.V., All rights reserved.

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AB - A novel plug-and-play setup based on polycapillary X-ray optics enables three-dimensional (3D) confocal X-ray fluorescence (XRF) and X-ray absorption spectroscopy down to 8 × 8 × 11 μm3 (17 keV) at the European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A. A complete description and analytical characterization is presented, together with two recently performed experimental cases. In Deep Earth diamond São Luiz-Frankfurt am Main 16, an olivine-rich inclusion was mapped with full 3D XRF elemental imaging. The preliminary tests on Iron Gall ink contained in an historical document, a letter from the court of King Philip II of Spain, reveal both the delicate nature of Iron Gall ink and the lack of Fe–Ni chemical bonding.

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JO - Analytical Chemistry

JF - Analytical Chemistry

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Bauters S, Tack P, Rudloff-Grund J, Banerjee D, Longo A, Van Silfhout R et al. Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A. Analytical Chemistry. 2018 Feb 6;90(3):2389-2394. Epub 2018 Jan 10. doi: 10.1021/acs.analchem.7b05110

Polycapillary Optics Based Confocal Micro X-ray Fluorescence and X-ray Absorption Spectroscopy Setup at The European Synchrotron Radiation Facility Collaborative Research Group Dutch–Belgian Beamline, BM26A

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