Quantitative nanosims analysis of grain boundary segregation in bulk samples

F Christien; C Downing; K L Moore; C R M Grovenor

Quantitative nanosims analysis of grain boundary segregation in bulk samples

F Christien
, C Downing
, K L Moore
, C R M Grovenor

Research output: Chapter in Book/Conference proceeding › Conference contribution

Abstract

Solute grain boundary (GB) segregation is an important metallurgical phenomenon that has been extensively studied over the last 40 years, especially by Auger spectroscopy of fractured surfaces. More recently, it has been demonstrated that High Resolution SIMS (NanoSIMS) analysis can detect solute GB segregation on a simple polished cross-section. The aim of the work presented here is to demonstrate the use of SIMS to achieve quantitative analysis of GB segregation.

Original language	English
Title of host publication	host publication
Pages	265-271
Number of pages	7
Volume	1
Publication status	Published - 2012
Event	141st Annual Meeting and Exhibition, TMS 2012 - Orlando, FL, United States Duration: 11 Mar 2012 → 15 Mar 2012 http://www.scopus.com/inward/record.url?eid=2-s2.0-84860865547&partnerID=40&md5=0bce687833020d9b73157a0c9ef5dfaa

Conference

Conference	141st Annual Meeting and Exhibition, TMS 2012
Country/Territory	United States
City	Orlando, FL
Period	11/03/12 → 15/03/12
Internet address	http://www.scopus.com/inward/record.url?eid=2-s2.0-84860865547&partnerID=40&md5=0bce687833020d9b73157a0c9ef5dfaa

Keywords

Auger Electron Spectroscopy (AES)
Microbeam techniques
SIMS
Surface analysis
Traces
Auger spectroscopy
Bulk samples
Fractured surfaces
Grain boundary segregation
High resolution
Microbeam technique
NanoSIMS
Auger electron spectroscopy
Exhibitions
Grain boundaries
Lunar surface analysis
Secondary ion mass spectrometry
Segregation (metallography)

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@inproceedings{129341962972462f86f0bd0f3dc55b0e,

title = "Quantitative nanosims analysis of grain boundary segregation in bulk samples",

abstract = "Solute grain boundary (GB) segregation is an important metallurgical phenomenon that has been extensively studied over the last 40 years, especially by Auger spectroscopy of fractured surfaces. More recently, it has been demonstrated that High Resolution SIMS (NanoSIMS) analysis can detect solute GB segregation on a simple polished cross-section. The aim of the work presented here is to demonstrate the use of SIMS to achieve quantitative analysis of GB segregation.",

keywords = "Auger Electron Spectroscopy (AES), Microbeam techniques, SIMS, Surface analysis, Traces, Auger spectroscopy, Bulk samples, Fractured surfaces, Grain boundary segregation, High resolution, Microbeam technique, NanoSIMS, Auger electron spectroscopy, Exhibitions, Grain boundaries, Lunar surface analysis, Secondary ion mass spectrometry, Segregation (metallography)",

author = "F Christien and C Downing and Moore, \{K L\} and Grovenor, \{C R M\}",

note = "Conference code: 89569 Export Date: 26 January 2015 CODEN: 85MVA Correspondence Address: Christien, F.; Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH, United Kingdom References: Lar{\`e}re, A., Guttmann, M., Dumoulin, P., Roques-Carmes, C., (1982) Acta Metall., 30, p. 685; Ben Mostepha, L., Saindrenan, G., Barbouth, N., Brass, A.M., Ch{\^e}ne, J., (1990) Scripta Metall. Mater., 24, p. 773; Seah, M.P., (1990) Auger and X-ray Photoelectron Spectroscopy, 1. , Wiley, New York; Karlsson, L., Norden, H., Odelius, H., (1988) Acta Metall., 36, p. 1; Gavrilov, K.L., Bennison, S.J., Mikeska, K.R., Levi-Setti, R., (1999) Acta Mater., 47, p. 4031; McIntyre, N.S., Huctwith, C.M., Taylor, K.F., Keating, E., Petersen, N.O., Brennenst{\"u}hl, A.M., (2002) Surf. Interface Anal., 33, p. 447; Lozano-Perez, S., Schr{\"o}der, M., Yamada, T., Terachi, T., English, C.A., Grovenor, C.R.M., (2008) Appl. Surf. Sci., 255, p. 1541; Valle, N., Drillet, J., Pic, A., Migeon, H.N., (2011) Surf. Interface Anal., 43, p. 573; McLean, D., (1957) Grain Boundaries in Metals, , Clarendon Press, Oxford; Vladimirov, A.B., Kaigorodov, V.N., Klotzman, S.M., Trakhtenberg, I.S., (1975) Fizika Metallov I Metallovedenie, 39, p. 319; Christien, F., Downing, C., Moore, K., Grovenor, C.R.M., (2011) Surf. Interface Anal., , submitted to; Lejcek, P., Rar, A., Hofmann, S., (2002) Surf. Interface Anal., 34, p. 375; 141st Annual Meeting and Exhibition, TMS 2012 ; Conference date: 11-03-2012 Through 15-03-2012",

year = "2012",

language = "English",

volume = "1",

pages = "265--271",

booktitle = "host publication",

url = "http://www.scopus.com/inward/record.url?eid=2-s2.0-84860865547\&partnerID=40\&md5=0bce687833020d9b73157a0c9ef5dfaa",

}

Christien, F, Downing, C, Moore, KL & Grovenor, CRM 2012, Quantitative nanosims analysis of grain boundary segregation in bulk samples. in host publication. vol. 1, pp. 265-271, 141st Annual Meeting and Exhibition, TMS 2012, Orlando, FL, United States, 11/03/12. <http://www.scopus.com/inward/record.url?eid=2-s2.0-84860865547&partnerID=40&md5=0bce687833020d9b73157a0c9ef5dfaa>

TY - GEN

T1 - Quantitative nanosims analysis of grain boundary segregation in bulk samples

AU - Christien, F

AU - Downing, C

AU - Moore, K L

AU - Grovenor, C R M

N1 - Conference code: 89569 Export Date: 26 January 2015 CODEN: 85MVA Correspondence Address: Christien, F.; Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH, United Kingdom References: Larère, A., Guttmann, M., Dumoulin, P., Roques-Carmes, C., (1982) Acta Metall., 30, p. 685; Ben Mostepha, L., Saindrenan, G., Barbouth, N., Brass, A.M., Chêne, J., (1990) Scripta Metall. Mater., 24, p. 773; Seah, M.P., (1990) Auger and X-ray Photoelectron Spectroscopy, 1. , Wiley, New York; Karlsson, L., Norden, H., Odelius, H., (1988) Acta Metall., 36, p. 1; Gavrilov, K.L., Bennison, S.J., Mikeska, K.R., Levi-Setti, R., (1999) Acta Mater., 47, p. 4031; McIntyre, N.S., Huctwith, C.M., Taylor, K.F., Keating, E., Petersen, N.O., Brennenstühl, A.M., (2002) Surf. Interface Anal., 33, p. 447; Lozano-Perez, S., Schröder, M., Yamada, T., Terachi, T., English, C.A., Grovenor, C.R.M., (2008) Appl. Surf. Sci., 255, p. 1541; Valle, N., Drillet, J., Pic, A., Migeon, H.N., (2011) Surf. Interface Anal., 43, p. 573; McLean, D., (1957) Grain Boundaries in Metals, , Clarendon Press, Oxford; Vladimirov, A.B., Kaigorodov, V.N., Klotzman, S.M., Trakhtenberg, I.S., (1975) Fizika Metallov I Metallovedenie, 39, p. 319; Christien, F., Downing, C., Moore, K., Grovenor, C.R.M., (2011) Surf. Interface Anal., , submitted to; Lejcek, P., Rar, A., Hofmann, S., (2002) Surf. Interface Anal., 34, p. 375

PY - 2012

Y1 - 2012

N2 - Solute grain boundary (GB) segregation is an important metallurgical phenomenon that has been extensively studied over the last 40 years, especially by Auger spectroscopy of fractured surfaces. More recently, it has been demonstrated that High Resolution SIMS (NanoSIMS) analysis can detect solute GB segregation on a simple polished cross-section. The aim of the work presented here is to demonstrate the use of SIMS to achieve quantitative analysis of GB segregation.

AB - Solute grain boundary (GB) segregation is an important metallurgical phenomenon that has been extensively studied over the last 40 years, especially by Auger spectroscopy of fractured surfaces. More recently, it has been demonstrated that High Resolution SIMS (NanoSIMS) analysis can detect solute GB segregation on a simple polished cross-section. The aim of the work presented here is to demonstrate the use of SIMS to achieve quantitative analysis of GB segregation.

KW - Auger Electron Spectroscopy (AES)

KW - Microbeam techniques

KW - SIMS

KW - Surface analysis

KW - Traces

KW - Auger spectroscopy

KW - Bulk samples

KW - Fractured surfaces

KW - Grain boundary segregation

KW - High resolution

KW - Microbeam technique

KW - NanoSIMS

KW - Auger electron spectroscopy

KW - Exhibitions

KW - Grain boundaries

KW - Lunar surface analysis

KW - Secondary ion mass spectrometry

KW - Segregation (metallography)

M3 - Conference contribution

VL - 1

SP - 265

EP - 271

BT - host publication

T2 - 141st Annual Meeting and Exhibition, TMS 2012

Y2 - 11 March 2012 through 15 March 2012

ER -

Quantitative nanosims analysis of grain boundary segregation in bulk samples

Abstract

Conference

Keywords

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