Rapid Natural-Abundance 2D13C-13C Correlation Spectroscopy Using Dynamic Nuclear Polarization Enhanced Solid-State NMR and Matrix-Free Sample Preparation

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Abstract

Ultra‐fast : Substantial solid‐state NMR sensitivity can be achieved using dynamic nuclear polarization and matrix‐free sample preparation (that is, absence of solvent and cryoprotectant). This method avoids line‐broadening, maximizes sample filling factor, and allows natural‐abundance 2D 13C–13C dipolar correlation experiments to be carried out in tens of minutes. MW=microwaves.
Original languageEnglish
Pages (from-to)11766-11769
Number of pages4
JournalAngewandte Chemie International Edition
Volume51
Issue number47
DOIs
Publication statusPublished - 19 Nov 2012

Keywords

  • 2D correlation
  • analytical methods
  • dynamic nuclear polarization
  • natural abundance
  • NMR spectroscopy

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