Sensitive absorptive refocused scalar correlation NMR spectroscopy in solids

Daniel Lee, Jochem Struppe, Douglas W. Elliott, Leonard J. Mueller, Jeremy J. Titman

Research output: Contribution to journalArticlepeer-review


A new two-dimensional NMR experiment is described which is suitable for obtaining magic angle spinning (MAS) scalar correlation spectra in solids. The new experiment has several advantages, including increased cross peak intensities, coupled with good suppression of the diagonal. Its utility is demonstrated via assignments of the carbon-13 MAS spectra of progesterone at natural abundance and of the polymer phase of 50%-U-13C-CsC60.
Original languageEnglish
Pages (from-to)3547-3553
Number of pages7
JournalPhysical Chemistry Chemical Physics
Issue number18
Publication statusPublished - 14 May 2009


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