Simultaneous measurement of X-ray powder diffraction and ferroelectric polarisation data as a function of applied electric field at a range of frequencies

Stephanie Ryding; Robert Cernik; Jenny Wooldridge; Timothy Burnett; Mark Stewart; Carlo Vecchini; Markys G Cain; Alistair Lennie; Fajin Yuan; Chiu Tang; Paul Thompson

doi:10.1017/s0885715613001024

Simultaneous measurement of X-ray powder diffraction and ferroelectric polarisation data as a function of applied electric field at a range of frequencies

Stephanie Ryding, Robert Cernik, Jenny Wooldridge, Timothy Burnett, Mark Stewart, Carlo Vecchini, Markys G Cain, Alistair Lennie, Fajin Yuan, Chiu Tang, Paul Thompson

Research output: Contribution to journal › Article › peer-review

Abstract

A variable frequency ferroelec. polarization measurement system was designed and built at the UK's Diamond Light Source. The elec. field induced phase transitions in Pb(Zr1-xTix)O3 (PZT) were used to test the facility via in-situ measurements of elec. polarization and XRD. Stroboscopic and real time data collection methods on polycryst. samples were employed as a function of frequency to det. the dynamic ferroelec. response. The system was shown to deliver XRD patterns of good statistical quality measured over 40 points of a ferroelec. PE loop. The system is now available on station I11 as a user facility at the Diamond Light Source. [on SciFinder(R)]

Original language	English
Pages (from-to)	S220-S227
Number of pages	8
Journal	Powder Diffr.
Volume	28
Issue number	S2
DOIs	https://doi.org/10.1017/s0885715613001024
Publication status	Published - Sept 2013

Keywords

Electric field effects
Phase transition (elec. field-induced phase transitions in lead zirconium titanate in relation to ferroelec. polarization)
Ferroelectricity
Powder x-ray diffraction (simultaneous measurement of x-ray powder diffraction and ferroelec. polarization data as a function of applied elec. field at a range of frequencies)
xray powder diffraction ferroelec polarization elec field frequency titanate

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10.1017/s0885715613001024

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Ryding, S., Cernik, R., Wooldridge, J., Burnett, T., Stewart, M., Vecchini, C., Cain, M. G., Lennie, A., Yuan, F., Tang, C., & Thompson, P. (2013). Simultaneous measurement of X-ray powder diffraction and ferroelectric polarisation data as a function of applied electric field at a range of frequencies. Powder Diffr., 28(S2), S220-S227. https://doi.org/10.1017/s0885715613001024

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title = "Simultaneous measurement of X-ray powder diffraction and ferroelectric polarisation data as a function of applied electric field at a range of frequencies",

abstract = "A variable frequency ferroelec. polarization measurement system was designed and built at the UK's Diamond Light Source. The elec. field induced phase transitions in Pb(Zr1-xTix)O3 (PZT) were used to test the facility via in-situ measurements of elec. polarization and XRD. Stroboscopic and real time data collection methods on polycryst. samples were employed as a function of frequency to det. the dynamic ferroelec. response. The system was shown to deliver XRD patterns of good statistical quality measured over 40 points of a ferroelec. PE loop. The system is now available on station I11 as a user facility at the Diamond Light Source. [on SciFinder(R)]",

keywords = "Electric field effects, Phase transition (elec. field-induced phase transitions in lead zirconium titanate in relation to ferroelec. polarization), Ferroelectricity, Powder x-ray diffraction (simultaneous measurement of x-ray powder diffraction and ferroelec. polarization data as a function of applied elec. field at a range of frequencies), xray powder diffraction ferroelec polarization elec field frequency titanate",

author = "Stephanie Ryding and Robert Cernik and Jenny Wooldridge and Timothy Burnett and Mark Stewart and Carlo Vecchini and Cain, {Markys G} and Alistair Lennie and Fajin Yuan and Chiu Tang and Paul Thompson",

note = "CAN 160:320826 Electric Phenomena 12626-81-2 (Lead titanium zirconium oxide (PbTi0-1Zr0-1O3)) Role: PEP (Physical, engineering or chemical process), PRP (Properties), PROC (Process) (simultaneous measurement of x-ray powder diffraction and ferroelec. polarization data as a function of applied elec. field at a range of frequencies)",

year = "2013",

month = sep,

doi = "10.1017/s0885715613001024",

language = "English",

volume = "28",

pages = "S220--S227",

journal = "Powder Diffr.",

issn = "0885-7156",

publisher = "International Centre for Diffraction Data",

number = "S2",

}

Ryding, S, Cernik, R, Wooldridge, J, Burnett, T, Stewart, M, Vecchini, C, Cain, MG, Lennie, A, Yuan, F, Tang, C & Thompson, P 2013, 'Simultaneous measurement of X-ray powder diffraction and ferroelectric polarisation data as a function of applied electric field at a range of frequencies', Powder Diffr., vol. 28, no. S2, pp. S220-S227. https://doi.org/10.1017/s0885715613001024

TY - JOUR

T1 - Simultaneous measurement of X-ray powder diffraction and ferroelectric polarisation data as a function of applied electric field at a range of frequencies

AU - Ryding, Stephanie

AU - Cernik, Robert

AU - Wooldridge, Jenny

AU - Burnett, Timothy

AU - Stewart, Mark

AU - Vecchini, Carlo

AU - Cain, Markys G

AU - Lennie, Alistair

AU - Yuan, Fajin

AU - Tang, Chiu

AU - Thompson, Paul

N1 - CAN 160:320826 Electric Phenomena 12626-81-2 (Lead titanium zirconium oxide (PbTi0-1Zr0-1O3)) Role: PEP (Physical, engineering or chemical process), PRP (Properties), PROC (Process) (simultaneous measurement of x-ray powder diffraction and ferroelec. polarization data as a function of applied elec. field at a range of frequencies)

PY - 2013/9

Y1 - 2013/9

N2 - A variable frequency ferroelec. polarization measurement system was designed and built at the UK's Diamond Light Source. The elec. field induced phase transitions in Pb(Zr1-xTix)O3 (PZT) were used to test the facility via in-situ measurements of elec. polarization and XRD. Stroboscopic and real time data collection methods on polycryst. samples were employed as a function of frequency to det. the dynamic ferroelec. response. The system was shown to deliver XRD patterns of good statistical quality measured over 40 points of a ferroelec. PE loop. The system is now available on station I11 as a user facility at the Diamond Light Source. [on SciFinder(R)]

AB - A variable frequency ferroelec. polarization measurement system was designed and built at the UK's Diamond Light Source. The elec. field induced phase transitions in Pb(Zr1-xTix)O3 (PZT) were used to test the facility via in-situ measurements of elec. polarization and XRD. Stroboscopic and real time data collection methods on polycryst. samples were employed as a function of frequency to det. the dynamic ferroelec. response. The system was shown to deliver XRD patterns of good statistical quality measured over 40 points of a ferroelec. PE loop. The system is now available on station I11 as a user facility at the Diamond Light Source. [on SciFinder(R)]

KW - Electric field effects

KW - Phase transition (elec. field-induced phase transitions in lead zirconium titanate in relation to ferroelec. polarization)

KW - Ferroelectricity

KW - Powder x-ray diffraction (simultaneous measurement of x-ray powder diffraction and ferroelec. polarization data as a function of applied elec. field at a range of frequencies)

KW - xray powder diffraction ferroelec polarization elec field frequency titanate

U2 - 10.1017/s0885715613001024

DO - 10.1017/s0885715613001024

M3 - Article

SN - 0885-7156

VL - 28

SP - S220-S227

JO - Powder Diffr.

JF - Powder Diffr.

IS - S2

ER -

Simultaneous measurement of X-ray powder diffraction and ferroelectric polarisation data as a function of applied electric field at a range of frequencies

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