Simultaneously enhancing spectral resolution and sensitivity in heteronuclear correlation NMR spectroscopy.

Liladhar Paudel; Ralph W Adams; Peter Kiraly; Juan Aguilar Malavia; Mohammadali Foroozandeh; Matt Cliff; Mathias Nilsson; Péter Sándor; Jonathan P Waltho; Gareth A Morris

doi:10.1002/anie.201305709

Simultaneously enhancing spectral resolution and sensitivity in heteronuclear correlation NMR spectroscopy.

Liladhar Paudel, Ralph W Adams, Peter Kiraly, Juan Aguilar Malavia, Mohammadali Foroozandeh, Matt Cliff, Mathias Nilsson, Péter Sándor, Jonathan P Waltho, Gareth A Morris

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Abstract

BIRD's eye view: Adding periodic BIRD J-refocusing (BIRD=bilinear rotation decoupling) to data acquisition in an HSQC experiment causes broadband homonuclear decoupling, giving a single signal for each proton chemical shift. This pure shift method improves both resolution and signal-to-noise ratio, without the need for special data processing.

Original language	English
Pages (from-to)	11616-11619
Number of pages	4
Journal	Angewandte Chemie (International ed. in English)
Volume	52
Issue number	44
DOIs	https://doi.org/10.1002/anie.201305709
Publication status	Published - 25 Oct 2013

Keywords

NMR spectroscopy
bilinear rotation decoupling
gHSQC
homonuclear decoupling
structure elucidation

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title = "Simultaneously enhancing spectral resolution and sensitivity in heteronuclear correlation NMR spectroscopy.",

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keywords = "NMR spectroscopy, bilinear rotation decoupling, gHSQC, homonuclear decoupling, structure elucidation",

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T1 - Simultaneously enhancing spectral resolution and sensitivity in heteronuclear correlation NMR spectroscopy.

AU - Paudel, Liladhar

AU - Adams, Ralph W

AU - Kiraly, Peter

AU - Aguilar Malavia, Juan

AU - Foroozandeh, Mohammadali

AU - Cliff, Matt

AU - Nilsson, Mathias

AU - Sándor, Péter

AU - Waltho, Jonathan P

AU - Morris, Gareth A

N1 - 304FO Times Cited:18 Cited References Count:32

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AB - BIRD's eye view: Adding periodic BIRD J-refocusing (BIRD=bilinear rotation decoupling) to data acquisition in an HSQC experiment causes broadband homonuclear decoupling, giving a single signal for each proton chemical shift. This pure shift method improves both resolution and signal-to-noise ratio, without the need for special data processing.

KW - NMR spectroscopy

KW - bilinear rotation decoupling

KW - gHSQC

KW - homonuclear decoupling

KW - structure elucidation

U2 - 10.1002/anie.201305709

DO - 10.1002/anie.201305709

M3 - Article

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SN - 1521-3773

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JO - Angewandte Chemie (International ed. in English)

JF - Angewandte Chemie (International ed. in English)

IS - 44

ER -

Simultaneously enhancing spectral resolution and sensitivity in heteronuclear correlation NMR spectroscopy.

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