Synthesis of the nickel selenophosphinates [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles

Weerakanya Maneeprakorn; Chinh Q. Nguyen; Mohammad A. Malik; Paul O'Brien; James Raftery

doi:10.1039/b816903a

Synthesis of the nickel selenophosphinates [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles

Weerakanya Maneeprakorn, Chinh Q. Nguyen, Mohammad A. Malik, Paul O'Brien, James Raftery

Research output: Contribution to journal › Article › peer-review

Abstract

Nickel phosphide (Ni2P and Ni12P5) or nickel selenide (NiSe) nanoparticles were prepared from the single molecule precursor, dialkyldiselenophosphinato nickel(II), [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) by thermolysis in trioctylphosphine oxide (TOPO) or hexadecylamine (HDA). The chemical composition of these nanoparticles depends on the precursors, capping agents, and reaction temperature. © 2009 The Royal Society of Chemistry.

Original language	English
Pages (from-to)	2103-2108
Number of pages	5
Journal	Dalton Transactions
Issue number	12
DOIs	https://doi.org/10.1039/b816903a
Publication status	Published - 2009

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10.1039/b816903a

CCDC 692536: Experimental Crystal Structure Determination
Maneeprakorn, W. (Contributor), Nguyen, C. Q. (Contributor), Malik, M. (Contributor), O'Brien, P. (Contributor) & Raftery, J. (Contributor), Cambridge Crystallographic Data Centre, 1 Jan 2009
DOI: 10.5517/ccr7mwg, http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccr7mwg&sid=DataCite
Dataset
CCDC 692535: Experimental Crystal Structure Determination
Maneeprakorn, W. (Contributor), Nguyen, C. Q. (Contributor), Malik, M. (Contributor), O'Brien, P. (Contributor) & Raftery, J. (Contributor), Cambridge Crystallographic Data Centre, 1 Jan 2009
DOI: 10.5517/ccr7mvf, http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccr7mvf&sid=DataCite
Dataset

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@article{05a5a5b6693f44e2bfa1b6458b3bedae,

title = "Synthesis of the nickel selenophosphinates [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles",

abstract = "Nickel phosphide (Ni2P and Ni12P5) or nickel selenide (NiSe) nanoparticles were prepared from the single molecule precursor, dialkyldiselenophosphinato nickel(II), [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) by thermolysis in trioctylphosphine oxide (TOPO) or hexadecylamine (HDA). The chemical composition of these nanoparticles depends on the precursors, capping agents, and reaction temperature. {\textcopyright} 2009 The Royal Society of Chemistry.",

author = "Weerakanya Maneeprakorn and Nguyen, {Chinh Q.} and Malik, {Mohammad A.} and Paul O'Brien and James Raftery",

note = "Times Cited: 12",

year = "2009",

doi = "10.1039/b816903a",

language = "English",

pages = "2103--2108",

journal = "Dalton Transactions",

issn = "1477-9234",

publisher = "Royal Society of Chemistry",

number = "12",

}

Synthesis of the nickel selenophosphinates [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles. / Maneeprakorn, Weerakanya; Nguyen, Chinh Q.; Malik, Mohammad A. et al.
In: Dalton Transactions, No. 12, 2009, p. 2103-2108.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Synthesis of the nickel selenophosphinates [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles

AU - Maneeprakorn, Weerakanya

AU - Nguyen, Chinh Q.

AU - Malik, Mohammad A.

AU - O'Brien, Paul

AU - Raftery, James

N1 - Times Cited: 12

PY - 2009

Y1 - 2009

N2 - Nickel phosphide (Ni2P and Ni12P5) or nickel selenide (NiSe) nanoparticles were prepared from the single molecule precursor, dialkyldiselenophosphinato nickel(II), [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) by thermolysis in trioctylphosphine oxide (TOPO) or hexadecylamine (HDA). The chemical composition of these nanoparticles depends on the precursors, capping agents, and reaction temperature. © 2009 The Royal Society of Chemistry.

AB - Nickel phosphide (Ni2P and Ni12P5) or nickel selenide (NiSe) nanoparticles were prepared from the single molecule precursor, dialkyldiselenophosphinato nickel(II), [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) by thermolysis in trioctylphosphine oxide (TOPO) or hexadecylamine (HDA). The chemical composition of these nanoparticles depends on the precursors, capping agents, and reaction temperature. © 2009 The Royal Society of Chemistry.

U2 - 10.1039/b816903a

DO - 10.1039/b816903a

M3 - Article

SN - 1477-9234

SP - 2103

EP - 2108

JO - Dalton Transactions

JF - Dalton Transactions

IS - 12

ER -

Synthesis of the nickel selenophosphinates [Ni(Se2PR 2)2] (R = iPr, tBu and Ph) and their use as single source precursors for the deposition of nickel phosphide or nickel selenide nanoparticles

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Datasets

CCDC 692536: Experimental Crystal Structure Determination

CCDC 692535: Experimental Crystal Structure Determination

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