The effect of temperature on viscosity of root canal sealers

Aim: To test the hypothesis that there was no significant (α = 0.05) change in viscosity of commercially available root canal sealers with increase in temperature using a high-performance Advanced Rheometric Expansion System (ARES) rheometer. Methodology: Materials tested were Apexit, Tubliseal EWT, Grossman's, AH Plus and Ketac-endo. Cone-and-plate geometry was used (25-mm diameter, 0.1 radian and gap 0.051 mm). Measurements were carried out for steady-state viscosity at 25 and 37°C in the shear rate range of 0.001-50 s-1 at standardized relative humidity and within 30 min from the start of mixing. Five samples were taken for each sealer at each temperature. Results: At 25°C all sealers demonstrated shear thinning. At 37°C Grossman's (powder : liquid ratio 2 : 1 and 3 : 1) and Ketac-endo had a rapid rise in viscosity and early set whereas the other sealers were shear thinning. On increasing temperature from 25°C to 37°C, Apexit, Tubliseal and AH Plus had reduced viscosity whereas Grossman's 2 : 1, Grossman's 3 : 1 and Ketac-endo had increased viscosity, which varied with the shear rate. The change in viscosity with change in temperature was significant (P <0.05) for all sealers except AH Plus. Conclusions: There was a variation in the effect of increasing temperature on each sealer depending on the shear rate. With the exception of AH Plus, a significant (P <0.05) change in viscosity was found, and the null hypothesis was rejected. © 2006 International Endodontic Journal.