The synthesis of iron sulfide nanocrystals from tris(O-alkylxanthato) iron(III) complexes

Masood Akhtar; Mohammad Azad Malik; Floriana Tuna; Paul O'Brien

doi:10.1039/c3ta12178j

The synthesis of iron sulfide nanocrystals from tris(O-alkylxanthato) iron(III) complexes

Masood Akhtar, Mohammad Azad Malik, Floriana Tuna, Paul O'Brien

Research output: Contribution to journal › Article › peer-review

Abstract

Tris(O-alkylxanthato)iron(iii) complexes (alkyl = Me (1), Et (2), and iBu (3)) were used as single source precursors for the synthesis of iron sulfide nanocrystals by thermolysis in oleylamine, hexadecylamine and octadecylamine at 170 to 300 °C. The morphology of the crystallites was strongly affected by the reaction conditions as well as the type of precursor used. © 2013 The Royal Society of Chemistry.

Original language	English
Pages (from-to)	8766-8774
Number of pages	8
Journal	Journal of Materials Chemistry A
Volume	1
Issue number	31
DOIs	https://doi.org/10.1039/c3ta12178j
Publication status	Published - 21 Aug 2013

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abstract = "Tris(O-alkylxanthato)iron(iii) complexes (alkyl = Me (1), Et (2), and iBu (3)) were used as single source precursors for the synthesis of iron sulfide nanocrystals by thermolysis in oleylamine, hexadecylamine and octadecylamine at 170 to 300 °C. The morphology of the crystallites was strongly affected by the reaction conditions as well as the type of precursor used. {\textcopyright} 2013 The Royal Society of Chemistry.",

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AU - Akhtar, Masood

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AU - Tuna, Floriana

AU - O'Brien, Paul

PY - 2013/8/21

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AB - Tris(O-alkylxanthato)iron(iii) complexes (alkyl = Me (1), Et (2), and iBu (3)) were used as single source precursors for the synthesis of iron sulfide nanocrystals by thermolysis in oleylamine, hexadecylamine and octadecylamine at 170 to 300 °C. The morphology of the crystallites was strongly affected by the reaction conditions as well as the type of precursor used. © 2013 The Royal Society of Chemistry.

U2 - 10.1039/c3ta12178j

DO - 10.1039/c3ta12178j

M3 - Article

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VL - 1

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JO - Journal of Materials Chemistry A

JF - Journal of Materials Chemistry A

IS - 31

ER -

The synthesis of iron sulfide nanocrystals from tris(O-alkylxanthato) iron(III) complexes

Abstract

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